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METHOD VALIDATION FOR DETERMINATION OF ORGANOCHLORINE PESTICIDE RESIDUES IN FOOD AND FEED
Vol. 8 No. 1 (2015), Original Research Articles
Vol. 8 No. 1 (2015)

METHOD VALIDATION FOR DETERMINATION OF ORGANOCHLORINE PESTICIDE RESIDUES IN FOOD AND FEED

Original Research Articles
https://doi.org/10.46784/e-avm.v8i1.105
Published 08.03.2016
Brankica Kartalović
Scientific Veterinary Institute “Novi Sad”, Novi Sad, Republic of Serbia
Željko Mihaljev
Scientific Veterinary Institute “Novi Sad”, Novi Sad, Republic of Serbia
Nadežda Prica
Scientific Veterinary Institute “Novi Sad”, Novi Sad, Republic of Serbia
Sandra Jakšić
Scientific Veterinary Institute “Novi Sad”, Novi Sad, Republic of Serbia
https://orcid.org/0000-0002-0799-1797
Milica Živkov Baloš
Scientific Veterinary Institute “Novi Sad”, Novi Sad, Republic of Serbia
Miroslav Ćirković
Scientific Veterinary Institute “Novi Sad”, Novi Sad, Republic of Serbia
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Keywords

validation
matrix
GC-MS
QuEChERS

How to Cite

Kartalović, B., Mihaljev, Željko, Prica, N., Jakšić, S., Živkov Baloš, M. and Ćirković, M. (2016) “METHOD VALIDATION FOR DETERMINATION OF ORGANOCHLORINE PESTICIDE RESIDUES IN FOOD AND FEED”, Archives of Veterinary Medicine, 8(1), pp. 37–46. doi: 10.46784/e-avm.v8i1.105.
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Abstract

Validation of analytical methods ensures the reliability and accuracy of analytical results. To get a reliable result we performed a validation of
the method taking into account all factors that may aff ect of the result. In this paper we optimized QuEChERS method for food and feed sample preparation as well as instrumental method using gas chromatography with mass spectrometry (GC-MS), and we obtained a method for successful determination of pesticides with calibration through the matrix. In this way, applying calibration through matrix, we satisfi ed the requirements for precision and reproducibility of the method being less than 20%, the accuracy rate in the range of 70-130% and method linearity throughout the range of interest.

https://doi.org/10.46784/e-avm.v8i1.105
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